4-Iodobenzenesulfonyl chloride → N-{3-Bromo-4-[(trifluoromethyl)oxy]phenyl}-4-iodobenzenesulfonamide

反応式

[Br:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[O:9][C:10]([F:13])([F:12])[F:11])[NH2:5].[I:14][C:15]1[CH:20]=[CH:19][C:18]([S:21](Cl)(=[O:23])=[O:22])=[CH:17][CH:16]=1>>[Br:1][C:2]1[CH:3]=[C:4]([NH:5][S:21]([C:18]2[CH:19]=[CH:20][C:15]([I:14])=[CH:16][CH:17]=2)(=[O:23])=[O:22])[CH:6]=[CH:7][C:8]=1[O:9][C:10]([F:11])([F:12])[F:13]

参加物

反応物 2

HCID 73994-Iodobenzenesulfonyl chloride

HCID 27364183-Bromo-4-(trifluoromethoxy)aniline

生成物 1

HCID 69197676N-{3-Bromo-4-[(trifluoromethyl)oxy]phenyl}-4-iodobenzenesulfonamide

実験手順

The title compound was prepared from 3-bromo-4-[(trifluoromethyl)oxy]aniline and 4-iodobenzenesulfonyl chloride using a similar method to that described for Examples 82-100. MS (ES−) m/e 520/522 [M−H]−.

出典と根拠

ORDレコード: ord-0dd80e35746f433e84dcd5192774e9f5
出典データセット: uspto-grants-2008_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07381728B2

反応ノート

読み込み中…