化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Peroxide → 3-(4-Formyl-phenoxymethyl)-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 3-[(4-Formylphenoxy)methyl]benzonitrile | HCID 17608676 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | 3-(4-Formyl-phenoxymethyl)-benzamide | HCID 47172831 | — |
反応手順
To a solution of 3-(4-Formyl-phenoxymethyl)benzonitrile (1 equiv), in DMSO was added potassium carbonate (0.5 equiv), and hydrogen peroxide (4 equiv). The reaction mixture stirred at room temperature for 2 hours. The reaction was monitored by TLC. It was poured on water and extracted with ethyl acetate (×3). The organic phase was dried over magnesium sulphate, filtered and concentrated under vacuum to yield a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07381750B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-b846b8b452874160bf4fee4b5eca3a8f |
| 出典メモ | uspto-grants-2008_06 |