戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 131341作成日:2026年10月26日

4-Chloro-2-nitroaniline → 2-(4-Chloro-2-nitro-phenylamino)-5-trifluoromethyl-benzonitrile

https://huagongshe.com/reaction/131341

反応式

関与物質

役割名称HCID仕込み量
反応物4-Chloro-2-nitroanilineHCID 6979—
反応物2-Fluoro-5-(trifluoromethyl)benzonitrileHCID 521016—
生成物2-(4-Chloro-2-nitro-phenylamino)-5-trifluoromethyl-benzonitrileHCID 5862599295%

反応手順

Using a method similar to Example 39, using 4-chloro-2-nitro-phenylamine (6.4 g, 37.3 mmol), 2-fluoro-5-trifluoromethyl-benzonitrile (7.05 g, 37.3 mmol) to obtain 12.03 g of the title compound (95% yield) as an amorphous yellow solid. Product can be used as is with no further purification: Mass Spectrum (m/e): 342(M+1).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07384934B2
出典データセットuspto-grants-2008_06
ORD IDord-3b5cb89fabd84709bb6d39d0840549fc
出典メモuspto-grants-2008_06