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4-Chloro-2-nitroaniline → 2-(4-Chloro-2-nitro-phenylamino)-5-trifluoromethyl-benzonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chloro-2-nitroaniline | HCID 6979 | — |
| 反応物 | 2-Fluoro-5-(trifluoromethyl)benzonitrile | HCID 521016 | — |
| 生成物 | 2-(4-Chloro-2-nitro-phenylamino)-5-trifluoromethyl-benzonitrile | HCID 58625992 | 95% |
反応手順
Using a method similar to Example 39, using 4-chloro-2-nitro-phenylamine (6.4 g, 37.3 mmol), 2-fluoro-5-trifluoromethyl-benzonitrile (7.05 g, 37.3 mmol) to obtain 12.03 g of the title compound (95% yield) as an amorphous yellow solid. Product can be used as is with no further purification: Mass Spectrum (m/e): 342(M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07384934B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-3b5cb89fabd84709bb6d39d0840549fc |
| 出典メモ | uspto-grants-2008_06 |