3-Phenoxyaniline → 2'-Methyl-5'-(5-methyl-1,3,4-oxadiazol-2-yl)-N-(3-phenoxyphenyl)-1,1'-biphenyl-4-carboxamide

HRID 131714

反応式

HRID 131714 の反応式
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]([CH3:13])=[N:11][N:12]=2)=[CH:4][C:3]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20](O)=[O:21])=[CH:16][CH:15]=1.[O:23]([C:30]1[CH:31]=[C:32]([CH:34]=[CH:35][CH:36]=1)[NH2:33])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:9][C:10]([CH3:13])=[N:11][N:12]=2)=[CH:4][C:3]=1[C:14]1[CH:15]=[CH:16][C:17]([C:20]([NH:33][C:32]2[CH:34]=[CH:35][CH:36]=[C:30]([O:23][C:24]3[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=3)[CH:31]=2)=[O:21])=[CH:18][CH:19]=1

参加物

3

反応物 2

HCID 771353-PhenoxyanilineHCID 112201194-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid

生成物 1

HCID 102764072'-Methyl-5'-(5-methyl-1,3,4-oxadiazol-2-yl)-N-(3-phenoxyphenyl)-1,1'-biphenyl-4-carboxamide

実験手順

2′-Methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-N-(3-phenoxyphenyl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 3-phenoxyaniline using method I. LCMS; retention time 3.85 min, MH+ 462.

出典と根拠

ORDレコード
ord-5683e03f99664012b354545afb289504
出典データセット
uspto-grants-2008_06
特許番号
US07384963B2

関連ノート

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