p-Bromoacetophenone → 1-(4-Bromophenyl)-3-(4-hydroxy-3,5-dimethylphenyl)prop-2-en-1-one

HRID 132084

反応式

HRID 132084 の反応式
[CH3:1][C:2]([C:4]1[CH:9]=[CH:8][C:7]([Br:10])=[CH:6][CH:5]=1)=[O:3].[CH3:11][C:12]1[CH:13]=[C:14]([CH:17]=[C:18]([CH3:21])[C:19]=1[OH:20])[CH:15]=O>>[Br:10][C:7]1[CH:8]=[CH:9][C:4]([C:2](=[O:3])[CH:1]=[CH:15][C:14]2[CH:17]=[C:18]([CH3:21])[C:19]([OH:20])=[C:12]([CH3:11])[CH:13]=2)=[CH:5][CH:6]=1

参加物

3

反応物 2

HCID 7466p-BromoacetophenoneHCID 752223,5-Dimethyl-4-hydroxybenzaldehyde

生成物 1

HCID 667042731-(4-Bromophenyl)-3-(4-hydroxy-3,5-dimethylphenyl)prop-2-en-1-one

実験手順

This compound was synthesized from 4-bromoacetophenone and 3,5-dimethyl-4-hydroxybenzaldehyde according to general method 1 described hereinabove. Purification was by silica gel chromatography (cyclohexane/ethyl acetate 90:10).

後処理

  1. customPurification

出典と根拠

ORDレコード
ord-3906a37d3bd1418d9dc08c12c25268f4
出典データセット
uspto-grants-2008_06
特許番号
US07385082B2

関連ノート

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