N-(2-(diethylamino)ethyl)-4-nitrosobenzamide → N-(2-(diethylamino)ethyl)-4-nitrosobenzamide

HRID 132507ノート

反応式

HRID 132507 の反応式
[CH3:1][CH2:2][N:3]([CH2:6][CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]=[O:18])=[CH:13][CH:12]=1)=[O:10])[CH2:4][CH3:5]>O>[CH3:5][CH2:4][N:3]([CH2:6][CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]=[O:18])=[CH:13][CH:12]=1)=[O:10])[CH2:2][CH3:1].[OH2:10].[CH3:5][CH2:4][N:3]([CH2:6][CH2:7][NH:8][C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]=[O:18])=[CH:13][CH:12]=1)=[O:10])[CH2:2][CH3:1]

参加物

4

反応物 1

HCID 125601N-(2-(diethylamino)ethyl)-4-nitrosobenzamide

生成物 2

HCID 125601N-(2-(diethylamino)ethyl)-4-nitrosobenzamideHCID 131726924HCID 131726924、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

The NOPA/water slurry was prepared by dispersing NOPA crystals in water under ambient conditions, and by oven-annealing the slurry in a closed container at a temperature of 70° C. for a time sufficient so as to yield a pourable, translucent, partial-solution of NOPA in water. NOPA was similarly mixed with IPA to yield a completely soluble solution at room temperature. The octanoic acid and NOS compounds were used as received in their neat liquid forms.

出典と根拠

ORDレコード
ord-0fc1fdf047c040b8a9ed9c3b8ce2627f
出典データセット
uspto-grants-2008_06
特許番号
US07387795B2

反応ノート

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