化工社化工社 化学情報印刷レポート · 研究参考用
3,5-Heptanedione → 2,6-Dimethyl-3,5-heptandiol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Heptanedione | HCID 81923 | — |
| 反応物 | 3,5-Heptanedione, 2,6-dimethyl- | HCID 87597 | — |
| 生成物 | 2,6-Dimethyl-3,5-heptandiol | HCID 13623112 | 90% |
反応手順
Synthesis procedure was similar to that described in synthetic example 19(1), except that 3,5-heptandione was replaced by 2,6-dimethyl-3,5-heptandione, and finally the product was purified by distilling under reduced pressure. 2,6-dimethyl-3,5-heptandiol as a colorless liquid was obtained with a yield of 90%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07388061B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-04ac086d882341f888b8d3d82bf35919 |
| 出典メモ | uspto-grants-2008_06 |