関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Methyl 4-hydrazinylbenzoate | HCID 408928 | — |
| 溶媒 | Sodium Acetate | HCID 517045 | — |
| 生成物 | Methyl 4-(2-acetylhydrazino)benzoate | HCID 12765612 | 115.7% |
反応手順
5.5 g of methyl 4-hydrazinobenzoate are dissolved in 38.2 ml of AcOH comprising 2.4 g of sodium acetate and the mixture is heated at 80° C. for 18 hours. The inorganic material is filtered off, the filtrate is then evaporated and the residue is taken up in the minimum amount of Et2O. The mixture is filtered to produce 7.97 g of the expected compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07390818B2 |
|---|
| 出典データセット | uspto-grants-2008_06 |
|---|
| ORD ID | ord-07f58774b4744ce2b08cb56ac6cf1c96 |
|---|
| 出典メモ | uspto-grants-2008_06 |
|---|
