化工社化工社 化学情報印刷レポート · 研究参考用
Isobutyl iodide → 1,3-dihydro-1-isobutyl-5-phenyl-2H-1,4-benzodiazepin-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutyl iodide | HCID 10556 | — |
| 反応物 | RO-05-2921 | HCID 76175 | — |
| 生成物 | 1,3-dihydro-1-isobutyl-5-phenyl-2H-1,4-benzodiazepin-2-one | HCID 22312025 | — |
反応手順
1,3-Dihydro-5-phenyl-2H-1,4-benzodiazepin-2-one (prepared according to the procedure of M. G. Bock et al., J. Org. Chem. 1987, 52, 3232-3239) was alkylated with isobutyl iodide using General Procedure 8-G to afford 1,3-dihydro-1-isobutyl-5-phenyl-2H-1,4-benzodiazepin-2-one.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07390801B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-130745f3862e46b4a7d3cb95f03b50b4 |
| 出典メモ | uspto-grants-2008_06 |