戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 133314作成日：2026年10月26日

3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine Iso-butyl Ester

https://huagongshe.com/reaction/133314

反応式

関与物質

役割名称HCID仕込み量
反応物3,4-DichloroanilineHCID 7257—
反応物Isobutyl pyruvateHCID 83084—
生成物N-(3,4-dichlorophenyl)alanine Iso-butyl EsterHCID 15434840—

反応手順

Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.55 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07390801B2
出典データセットuspto-grants-2008_06
ORD IDord-9f1db41788c449c3a90acf91524b0cb7
出典メモuspto-grants-2008_06