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HRID 133316作成日：2026年10月26日

3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine n-butyl Ester

https://huagongshe.com/reaction/133316

反応式

関与物質

役割名称HCID仕込み量
反応物3,4-DichloroanilineHCID 7257—
反応物Butyl pyruvateHCID 523883—
生成物N-(3,4-dichlorophenyl)alanine n-butyl EsterHCID 53854721—

反応手順

Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and n-butyl pyruvate (prepared by following General Procedure AO above using n-butanol in place of iso-butanol), the title compound was prepared. The reaction was monitored by tlc on silica gel (Rf=0.7 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07390801B2
出典データセットuspto-grants-2008_06
ORD IDord-ebbab71237274d50a9ae2a032dfefe5c
出典メモuspto-grants-2008_06