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HRID 133331作成日：2026年10月27日

3,5-Dichloroaniline → N-(3,5-dichlorophenyl)alanine isobutyl ester

https://huagongshe.com/reaction/133331

反応式

関与物質

役割名称HCID仕込み量
反応物3,5-DichloroanilineHCID 12281—
反応物Isobutyl pyruvateHCID 83084—
生成物N-(3,5-dichlorophenyl)alanine isobutyl esterHCID 54461425—

反応手順

Following General Procedure AA above and using 3,5-dichloroaniline (Aldrich) and isobutyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07390801B2
出典データセットuspto-grants-2008_06
ORD IDord-8837b08adeb74b129b8749ac560c28d2
出典メモuspto-grants-2008_06