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HRID 133352作成日：2026年10月26日

Benzenepropanoyl chloride → N-(3-phenylpropionyl)-D,L-alanine Isobutyl Ester

https://huagongshe.com/reaction/133352

反応式

関与物質

役割名称HCID仕込み量
反応物Benzenepropanoyl chlorideHCID 64801—
反応物2-Methylpropyl 2-aminopropanoate hydrochlorideHCID 86200109—
生成物N-(3-phenylpropionyl)-D,L-alanine Isobutyl EsterHCID 15480461—

反応手順

Following General Procedure BA above and using 3-phenylpropionyl chloride (Aldrich) and D,L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as a solid having a melting point of from 511-54° C. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07390801B2
出典データセットuspto-grants-2008_06
ORD IDord-8fe1a45c8bc241b2b54d32eee6407036
出典メモuspto-grants-2008_06