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Benzenepentanoic acid → N-(5Phenylpentanoyl)-L-alanine iso-Butyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenepentanoic acid | HCID 16757 | — |
| 反応物 | 2-Methylpropyl (2S)-2-aminopropanoate hydrochloride | HCID 86584981 | — |
| 生成物 | N-(5Phenylpentanoyl)-L-alanine iso-Butyl Ester | HCID 15481770 | — |
反応手順
Following General Procedure BB and using 5-phenylpentanoic acid (Aldrich) and L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07390801B2 |
| 出典データセット | uspto-grants-2008_06 |
| ORD ID | ord-4716790d131b4023936be71dfd4aa640 |
| 出典メモ | uspto-grants-2008_06 |