関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethylformamide | HCID 6228 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4-(Methylsulfonyl)phenol | HCID 123350 | — |
| 反応物 | 4-Bromo-5-fluoro-2-nitroaniline | HCID 21911928 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Bromo-5-(4-methanesulfonyl-phenoxy)-2-nitro-phenylamine | HCID 23145228 | — |
反応手順
5.2 g of 4-methanesulfonyl-phenol and 5.7 g of potassium carbonate were added in order to an N,N-dimethylformamide (50 ml) solution of 6.4 g of 4-bromo-5-fluoro-2-nitrophenylamine, and the reaction liquid was stirred at 120° C. for 3 hours. 200 ml of water was added to the reaction liquid, and the precipitated solid was taken out through filtration and dried to obtain the entitled compound as a brown solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07728025B2 |
|---|
| 出典データセット | uspto-grants-2010_06 |
|---|
| ORD ID | ord-2db425b5a31749ebb865df94ca6c54f9 |
|---|
| 出典メモ | uspto-grants-2010_06 |
|---|
