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HRID 1349133作成日：2026年10月27日

3-Amino-9-ethylcarbazole → (2S,4EZ)-4-(tert-butoxyimino)-1-(2-ethoxy-1-naphthoyl)-N-(9-ethyl-9H-carbazol-3-yl)-2-pyrrolidinecarboxamide

https://huagongshe.com/reaction/1349133

反応式

関与物質

役割名称HCID仕込み量
反応物3-Amino-9-ethylcarbazoleHCID 8588—
反応物1-Naphthalenecarbonyl chloride, 2-ethoxy-HCID 108679—
反応物(2S,4EZ)-1-(tertbutoxycarbonyl)-4-(tert-butoxyimino)-2-pyrrolidinecarboxylic acidHCID 131725425—
生成物(2S,4EZ)-4-(tert-butoxyimino)-1-(2-ethoxy-1-naphthoyl)-N-(9-ethyl-9H-carbazol-3-yl)-2-pyrrolidinecarboxamideHCID 131725486—

反応手順

Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(tert-butoxyimino)-2-pyrrolidinecarboxylic acid, 2-ethoxy-1-naphthoyl chloride, and 9-ethyl-9H-carbazol-3-amine the title compound was obtained in 47% purity by LC/MS. MS(ESI+): m/z=591.4.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07211601B2
出典データセットuspto-grants-2007_05
ORD IDord-49ba54081f96497a97adc21c6b2c92d8
出典メモuspto-grants-2007_05