HCID 86598976、化合物 → 2-[(2,5-Dichlorophenyl)thio]-2-phenylethylamine hydrochloride
反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][C:3]=1[S:9][CH:10]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[CH2:11][NH:12]C(=O)OC(C)(C)C>Cl.O1CCOCC1>[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][C:3]=1[S:9][CH:10]([C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=1)[CH2:11][NH2:12]参加物
4
実験手順
The product from step (b) (0.4 g) was dissolved in 4M HCl in dioxane (5 ml). The resulting solution was stirred at room temperature for 6 h, the solvent was evaporated and the residue triturated with ethyl acetate to give of the title compound (0.24 g) as, a white solid.
後処理
- customthe solvent was evaporated
- customthe residue triturated with ethyl acetate
出典と根拠
- ORDレコード
- ord-068525873f0548958249a87c4e0f4ad0
- 出典データセット
- uspto-grants-2007_05
- 特許番号
- US07223794B2
反応ノート
読み込み中…