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Methyl Ethyl Ketone → Ethanol heptane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl Ethyl Ketone | HCID 6569 | — |
| 反応物 | Hydralazine Hydrochloride | HCID 9351 | — |
| 溶媒 | Methanol--water (1/1) | HCID 22242641 | — |
| 生成物 | Ethanol heptane | HCID 22502148 | 78% |
反応手順
A 10 parts 1-hydrazinophthalazine HCL (0.05 Molar) in 50% methanol-water are mixed with 1 part 2-butanone. After evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone is crystallized from ethanol-heptane (78% yield). [The Journal of Pharmacology and Experimental Therapeutics 205 (2): 418-425 (1978)].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728133B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-38722a7553584aeca29efcd3a8985b6f |
| 出典メモ | uspto-grants-2010_06 |