Ammonium Hydroxide → HCID 18506197、化合物

反応式

[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[C:10](=[O:14])[NH:9][C:8]2=[O:15].[OH-].[NH4+:21]>>[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]([C:8]([NH2:21])=[O:15])[C:11](=[CH:12][CH:13]=1)[C:10]([NH2:9])=[O:14]

参加物

反応物 2

HCID 14923Ammonium Hydroxide

HCID 18506076HCID 18506076、化合物

生成物 1

HCID 18506197HCID 18506197、化合物

実験手順

5-(2-Aminophenoxy)-isoindole-1,3-dione (0.1 g, 0.38 mmol) in conc. ammonium hydroxide (aq) was stirred at 60° C. for two hours. The reaction mixture was evaporated in vacuo (cold in order not to make the imide again). The crude mixture was used without any purification.

後処理

customThe reaction mixture was evaporated in vacuo (cold in order not
customThe crude mixture was used without any purification

出典と根拠

ORDレコード: ord-fc642962978f4fe8bbdcf534f802d180
出典データセット: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06590118B1

反応ノート

読み込み中…

参加物