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HRID 1357750作成日:2026年10月27日

2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde

https://huagongshe.com/reaction/1357750

反応式

関与物質

役割名称HCID仕込み量
反応物2,1,3-Benzothiadiazol-5-ylmethanolHCID 2776294—
触媒HCID 178418406HCID 178418406—
溶媒ChloroformHCID 6212—
生成物2,1,3-Benzothiadiazole-5-carbaldehydeHCID 277629072.3%

反応手順

5-Hydroxymethylbenzo-2, 1,3-thiadiazole (2.6 g, 16 mmol) and manganese dioxide (6.0 g, 64 mmol) in chloroform (150 mL) were stirred at room temperature overnight. The reaction mixture was filtered off and the filtrate was evaporated to provide 1.9 g of the title compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06593335B1
出典データセットuspto-grants-2003_07
ORD IDord-d6214540b07f41f691e40f83b9cf0f40
出典メモuspto-grants-2003_07