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HRID 1359265作成日:2026年10月27日

Hydrogen Bromide → HCID 178515992、化合物

https://huagongshe.com/reaction/1359265

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrogen BromideHCID 260—
反応物2-Benzyl-6-methoxypyridineHCID 21942274—
溶媒WaterHCID 962—
生成物HCID 178515992HCID 17851599270.9%

反応手順

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring for 7 hours in an oil bath kept at 100° C. After cooling as it was, 250 ml of water was added thereto, and the resulting crystals were collected by filtration, washed with water and vacuum-dried, to give 38.9 g of the target compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06599917B1
出典データセットuspto-grants-2003_07
ORD IDord-05486037a3b44e6cb1ec2598db258d0c
出典メモuspto-grants-2003_07