化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Bromide → HCID 178515992、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 2-Benzyl-6-methoxypyridine | HCID 21942274 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178515992 | HCID 178515992 | 70.9% |
反応手順
A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring for 7 hours in an oil bath kept at 100° C. After cooling as it was, 250 ml of water was added thereto, and the resulting crystals were collected by filtration, washed with water and vacuum-dried, to give 38.9 g of the target compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06599917B1 |
| 出典データセット | uspto-grants-2003_07 |
| ORD ID | ord-05486037a3b44e6cb1ec2598db258d0c |
| 出典メモ | uspto-grants-2003_07 |