関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 2,4,5-Trifluorobenzoyl chloride | HCID 145164 | — |
| 反応物 | Ethyl 3-(cyclopentylamino)buta-2-enoate | HCID 66962611 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | HCID 178472172 | HCID 178472172 | — |
反応手順
Under ice cooling, triethylamine and 2,4,5-trifluorobenzoyl chloride were added to a solution of ethyl 3-(cyclopentylamino)buta-2-enoate in dioxane, for stirring at ambient temperature for 30 minutes and at 65° C. for one hour, to obtain ethyl 3-(cyclopentylamino)-2-(2,4,5-trifluorobenzoyl)buta-2-enoate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07879878B2 |
|---|
| 出典データセット | uspto-grants-2011_02 |
|---|
| ORD ID | ord-df21facae4124dc9a58d3d1110403fd7 |
|---|
| 出典メモ | uspto-grants-2011_02 |
|---|
