関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Pentacene | HCID 8671 | — |
| 反応物 | Maleimide | HCID 10935 | — |
| 溶媒 | 1,4-Dichlorobenzene | HCID 4685 | — |
| 生成物 | Pentacene maleimide | HCID 86643198 | — |
反応手順
A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07883685B1 |
|---|
| 出典データセット | uspto-grants-2011_02 |
|---|
| ORD ID | ord-85a1356c52bd41e4b4121d9a7f96ffc1 |
|---|
| 出典メモ | uspto-grants-2011_02 |
|---|
