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Isopropylamine → 2-Amino-N-isopropylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isopropylamine | HCID 6363 | — |
| 反応物 | Isatoic Anhydride | HCID 8359 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-Amino-N-isopropylbenzamide | HCID 94411 | 77.1% |
反応手順
A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07884098B2 |
| 出典データセット | uspto-grants-2011_02 |
| ORD ID | ord-7fc24b27a8664e549d66df96405fa8cf |
| 出典メモ | uspto-grants-2011_02 |