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L-Tryptophan → L-(-)-Tryptophanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | L-Tryptophan | HCID 6305 | — |
| 溶媒 | Methan(2H)ol | HCID 123113 | — |
| 生成物 | L-(-)-Tryptophanol | HCID 6951149 | 92% |
反応手順
The title compound was prepared from (S)-tryptophan according to Method D and was isolated as a solid in 92% yield. δH (MeOD-d3) 7.46 (1H, d, J 7.9 Hz), 7.21 (1H, d, J 8.0 Hz), 6.96 (3H, m), 3.79 (1H, dd, J 11.3 and 3.6 Hz), 3.54 (1H, dd, J 11.3 and 6.2 Hz), 3.05 (1H, m), 2.80 (1H, m), 2.61 (1H, m). Note: exchangeable protons not evident in MeOD.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07888344B2 |
| 出典データセット | uspto-grants-2011_02 |
| ORD ID | ord-007bb295874144248d771a25b8014a86 |
| 出典メモ | uspto-grants-2011_02 |