化工社化工社 化学情報印刷レポート · 研究参考用
Oxalyl chloride → (2,5-Dimethoxyphenyl)acetyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | 2,5-Dimethoxyphenylacetic acid | HCID 74469 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | (2,5-Dimethoxyphenyl)acetyl chloride | HCID 596088 | — |
反応手順
To a solution of 196 mg (1.00 mmol) of (2,5-dimethoxyphenyl)acetic acid in 3 mL of CH2Cl2 was added 100 μL of oxalyl chloride. The mixture was stirred at ambient temperature for 1 hour then concentrated under reduced pressure to a thick liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07888374B2 |
| 出典データセット | uspto-grants-2011_02 |
| ORD ID | ord-5f39d295ad2548daab8b070d6410a14a |
| 出典メモ | uspto-grants-2011_02 |