Oxalyl chloride → (2,5-Dimethoxyphenyl)acetyl chloride

HRID 1364528

反応式

HRID 1364528 の反応式
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([O:9][CH3:10])=[CH:5][C:4]=1[CH2:11][C:12]([OH:14])=O.C(Cl)(=O)C([Cl:18])=O>C(Cl)Cl>[O:2]([C:3]1[CH:8]=[CH:7][C:6]([O:9][CH3:10])=[CH:5][C:4]=1[CH2:11][C:12]([Cl:18])=[O:14])[CH3:1]

参加物

4

反応物 2

HCID 65578Oxalyl chlorideHCID 744692,5-Dimethoxyphenylacetic acid

生成物 1

HCID 596088(2,5-Dimethoxyphenyl)acetyl chloride

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

To a solution of 196 mg (1.00 mmol) of (2,5-dimethoxyphenyl)acetic acid in 3 mL of CH2Cl2 was added 100 μL of oxalyl chloride. The mixture was stirred at ambient temperature for 1 hour then concentrated under reduced pressure to a thick liquid.

後処理

  1. concentrationthen concentrated under reduced pressure to a thick liquid

出典と根拠

ORDレコード
ord-5f39d295ad2548daab8b070d6410a14a
出典データセット
uspto-grants-2011_02
特許番号
US07888374B2

関連ノート

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