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4-Chloro-3-(pyridin-2-yl)aniline → N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(ethylsulfonylmethyl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chloro-3-(pyridin-2-yl)aniline | HCID 40151925 | — |
| 反応物 | 4-(Ethylsulfonylmethyl)benzoic acid | HCID 43444445 | — |
| 生成物 | N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(ethylsulfonylmethyl)benzamide | HCID 58614777 | — |
反応手順
50 mg of 4-(ethylsulfonylmethyl)benzoic acid was coupled with 67 mg of 4-chloro-3-(pyridin-2-yl)aniline via Procedure G. This product was recrystallized from methanol to yield N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(ethylsulfonylmethyl)benzamide. MS (Q1) 415 (M)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07888364B2 |
| 出典データセット | uspto-grants-2011_02 |
| ORD ID | ord-94d0289438c944aea47a39dc9393e44c |
| 出典メモ | uspto-grants-2011_02 |