反応式
C1([S:7]([NH2:10])(=[O:9])=[O:8])CCCCC1.[CH2:11]([Mg]Cl)[C:12]([CH3:15])([CH3:14])[CH3:13]>C(OCC)C>[CH2:11]([S:7]([NH2:10])(=[O:9])=[O:8])[C:12]([CH3:15])([CH3:14])[CH3:13]参加物
4
実験手順
Following the procedure for the preparation of cyclohexylsulfonamide, 49 mL (37 mmol) of 0.75M neopentylmagnesium chloride (Alfa) in diethyl ether was converted to 1.52 g (27%) of the desired product as a white solid. 1H NMR (CDCl3) δ 1.17 (s, 9H), 3.12 (s, 2H), 4.74 (brs, 2H); 13C NMR (CDCl3) δ 29.46, 31.51, 67.38; MS m/e 150 (M−1)−.
出典と根拠
- ORDレコード
- ord-80a4c0f6e45e40c887f0c3d28f8e133d
- 出典データセット
- uspto-grants-2011_02
- 特許番号
- US07888464B2
関連ノート
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