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HRID 1371233作成日:2026年10月27日

Isopropenyl acetate → (+)-Styrallyl acetate

https://huagongshe.com/reaction/1371233

反応式

関与物質

役割名称HCID仕込み量
反応物Isopropenyl acetateHCID 7916—
反応物4-Chlorophenyl AcetateHCID 13410—
生成物(+)-Styrallyl acetateHCID 695170495%

反応手順

The procedure of Example 1 was repeated except that 3 molar equivalents of p-chlorophenyl acetate (a conventional acylating agent) was used in place of isopropenyl acetate in the presence of three times the amount of the enzyme catalyst used in Example 1 over a reaction period of 42 hours, to obtain (R)-1-phenylethyl acetate having an optical purity of higher than 99%, at a yield of 95%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07156731B2
出典データセットuspto-grants-2007_01
ORD IDord-1bc0273f6d9e4898b5a2d888224182f6
出典メモuspto-grants-2007_01