化工社化工社 化学情報印刷レポート · 研究参考用
Dimethylsulphamoyl chloride → 7-Dimethylsulfamoyl-3-(1-ethyl-5-fluoro-indan-1-yl)-1H-indole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylsulphamoyl chloride | HCID 83372 | — |
| 反応物 | 3-(1-Ethyl-5-fluoro-indan-1-yl)-1H-indol-7-ylamine | HCID 58941707 | — |
| 生成物 | 7-Dimethylsulfamoyl-3-(1-ethyl-5-fluoro-indan-1-yl)-1H-indole | HCID 68585458 | — |
反応手順
Utilizing 3-(1-ethyl-5-fluoro-indan-1-yl)-1H-indol-7-ylamine and dimethyl sulfamoyl chloride, the title compound is prepared as in example 15. 0.16 g (29%). LC-MS m/z 402.1 (M++1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728150B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-0630b0abd04f4f82a35413fda4e1b080 |
| 出典メモ | uspto-grants-2010_06 |