化工社化工社 化学情報印刷レポート · 研究参考用
Ethinylestradiol → Ethinyl Estradiol beta-cyclodextrin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethinylestradiol | HCID 5991 | — |
| 反応物 | beta-Cyclodextrin | HCID 444041 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Ethinyl Estradiol beta-cyclodextrin | HCID 10214247 | — |
反応手順
Process 2 (P2): Ethinyl estradiol is dissolved in acetone. β-cyclodextrin is dissolved at 45 C in water. The ethinyl estradiol solution is added to the beta-cyclodextrin solution. The obtained suspension is stirred for some hours at temperatures below 25° C. Afterwards, the crystallization product is isolated and dried by methods described infra.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07163931B2 |
| 出典データセット | uspto-grants-2007_01 |
| ORD ID | ord-3b956d393c104f7e92bd29215fe087a7 |
| 出典メモ | uspto-grants-2007_01 |