2,3-Dichloro-5-hydroxypyridine → 2-(5,6-dichloro-3-pyridyloxy)-N-(4-methylpent-2-yn-4-yl)butyramide

HRID 1374904ノート

反応式

HRID 1374904 の反応式
[Cl:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[N:6][C:7]=1[Cl:8].Br[CH:11]([CH2:21][CH3:22])[C:12]([NH:14][C:15]([CH3:20])([CH3:19])[C:16]#[C:17][CH3:18])=[O:13]>>[Cl:1][C:2]1[CH:3]=[C:4]([O:9][CH:11]([CH2:21][CH3:22])[C:12]([NH:14][C:15]([CH3:20])([CH3:19])[C:16]#[C:17][CH3:18])=[O:13])[CH:5]=[N:6][C:7]=1[Cl:8]

参加物

3

反応物 2

HCID 143916722,3-Dichloro-5-hydroxypyridineHCID 210784062-bromo-N-(4-methylpent-2-yn-4-yl)butyramide

生成物 1

HCID 210783702-(5,6-dichloro-3-pyridyloxy)-N-(4-methylpent-2-yn-4-yl)butyramide

実験手順

5,6-Dichloropyridin-3-ol was reacted with 2-bromo-N-(4methylpent-2-yn-4-yl)butyramide in a similar procedure to that described in Example 10, Stage 2 to give 2-(5,6-dichloro-3-pyridyloxy)-N-(4methylpent-2-yn-4-yl)butyramide, gum.

出典と根拠

ORDレコード
ord-e18f7b873f9244578e7e8fc7900561b3
出典データセット
uspto-grants-2007_01
特許番号
US07166621B2

反応ノート

読み込み中…