Methanol → Methyl 3,5-dichloro-4-methylbenzoate

反応式

[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Cl:12])[C:10]=1[CH3:11])[C:5]([OH:7])=[O:6].[CH3:13]O>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Cl:12])[C:10]=1[CH3:11])[C:5]([O:7][CH3:13])=[O:6]

参加物

反応物 2

HCID 887Methanol

HCID 185332343,5-Dichloro-4-methylbenzoic acid

生成物 1

HCID 10130655Methyl 3,5-dichloro-4-methylbenzoate

実験手順

This compound was prepared in the same manner as in Reference Example 1 (step 1), except that 3,5-dichloro-4-methylbenzoic acid (Japanese Unexamined Patent Publication (Kokai) No. 6-192196) was used and methanol was used as the solvent, and that the crude product was purified by silica gel column chromatography.

後処理

customthat the crude product was purified by silica gel column chromatography

出典と根拠

ORDレコード: ord-e51b2b92542745ac848a958d9fc03db1
出典データセット: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07728131B2

反応ノート

読み込み中…

参加物