1,3-Dioxan-5-one → 2,2-Dimethyl-1,3-dioxan-5-one

HRID 1376900ノート

反応式

HRID 1376900 の反応式
O1CC(=O)COC1.[CH2:8]([C:10]1([CH2:17]C)[O:15][CH2:14][C:13](=[O:16])[CH2:12][O:11]1)C.O1C2(CCCCC2)OCC(=O)C1>>[CH3:8][C:10]1([CH3:17])[O:15][CH2:14][C:13](=[O:16])[CH2:12][O:11]1

参加物

4

反応物 3

HCID 97937071,3-Dioxan-5-oneHCID 113212061,5-dioxaspiro[5.5]undecan-3-oneHCID 19078650HCID 19078650、化合物

生成物 1

HCID 27331412,2-Dimethyl-1,3-dioxan-5-one

実験手順

By working in a similar way but using 1,3-dioxan-5-one, 2,2-diethyl-1,3-dioxan-5-one and 1,5-dioxaspiro[5,5]undecan-3-one, in place of 2,2-dimethyl-1,3-dioxan-5-one, the following compounds were respectively obtained: 1,3-dioxan-5-one oxime, 2,2-diethyl-1,3-dioxan-5-one oxime and 1,5-dioxaspiro[5,5]undecan-3-one oxime.

出典と根拠

ORDレコード
ord-91af62f6bed24581a912f9985eb7dbbb
出典データセット
uspto-grants-1997_09
特許番号
US05663372

反応ノート

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