化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Bicarbonate → (S)-Benzyl piperidine-2-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | Benzyl piperidine-2-carboxylate | HCID 12436232 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | (S)-Benzyl piperidine-2-carboxylate | HCID 12436231 | — |
反応手順
Benzyl pipecolate was routinely generated by treating an ethyl acetate suspension of this salt with saturated sodium bicarbonate until dissolution of the organic material. The aqueous layer was extracted twice with ethyl acetate and the combined organic extracts were dried with MgSO4 and evaporated to yield (S)-Benzyl pipecolate (15) as a pale yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05665774 |
| 出典データセット | uspto-grants-1997_09 |
| ORD ID | ord-d97a83adc86d4fec85c6e1e641d731c5 |
| 出典メモ | uspto-grants-1997_09 |