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Benzyl Bromide → N-benzyl-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)hydroxylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Bromide | HCID 7498 | — |
| 反応物 | 1,2,2,6,6-Pentamethyl-piperidin-4-one oxime | HCID 241950 | — |
| 生成物 | N-benzyl-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)hydroxylamine | HCID 22902720 | 40% |
反応手順
Following the procedure of Example 1, the title compound is prepared from 1,2,2,6,6-pentamethylpiperidin-4-one oxime (5.0 g, 27 mmol) and benzyl bromide (4.6 g, 27 mmol) in a 40% yield to give 3.0 g of a white solid which melts at 107°-108° C. after recrystallization from ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05668198 |
| 出典データセット | uspto-grants-1997_09 |
| ORD ID | ord-8b77997329644ab3846141c875533c57 |
| 出典メモ | uspto-grants-1997_09 |