4-(Hydroxymethyl)benzaldehyde → 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde

HRID 1378633

反応式

HRID 1378633 の反応式
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[OH:16][CH2:17][C:18]1[CH:25]=[CH:24][C:21]([CH:22]=[O:23])=[CH:20][CH:19]=1>>[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8]([O:23][CH2:22][C:21]1[CH:24]=[CH:25][C:18]([CH:17]=[O:16])=[CH:19][CH:20]=1)=[O:9])([CH3:4])([CH3:3])[CH3:2]

参加物

3

反応物 2

HCID 5563304-(Hydroxymethyl)benzaldehydeHCID 136335553-Tert-butyl-4-methoxybenzoyl chloride

生成物 1

HCID 214745254-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde

実験手順

In a manner similar to Example 1(d), by reaction of 7.6 g (34 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 4.6 g (34 mmol) of 4-hydroxymethylbenzaldehyde, 5.6 g (51%) of the expected aldehyde, melting point 75°-6° C., are obtained.

後処理

  1. customare obtained

出典と根拠

ORDレコード
ord-90a3e7b3c5b54bf8ad6c72fa60aef757
出典データセット
uspto-grants-1997_09
特許番号
US05668156

関連ノート

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