2-Aminopyrimidine-4-carbaldehyde → 2-Aminopyrimidine-4-carboxaldehyde (1-carboxyethyl-4-piperidinyl)imine

反応式

[NH2:1][C:2]1[N:7]=[C:6]([CH:8]=O)[CH:5]=[CH:4][N:3]=1.[C:10]([CH:13]([N:15]1[CH2:20][CH2:19][CH:18]([NH2:21])[CH2:17][CH2:16]1)[CH3:14])([OH:12])=[O:11]>>[C:10]([CH:13]([N:15]1[CH2:16][CH2:17][CH:18]([N:21]=[CH:8][C:6]2[CH:5]=[CH:4][N:3]=[C:2]([NH2:1])[N:7]=2)[CH2:19][CH2:20]1)[CH3:14])([OH:12])=[O:11]

参加物

反応物 2

HCID 178323462-Aminopyrimidine-4-carbaldehyde

HCID 220025081-Carboxyethyl-4-aminopiperidine

生成物 1

HCID 867501672-Aminopyrimidine-4-carboxaldehyde (1-carboxyethyl-4-piperidinyl)imine

実験手順

2-Aminopyrimidine-4-carboxaldehyde and 1-carboxyethyl-4-aminopiperidine were reacted by the procedure of example 1(c) to afford the title compound as a yellow oil.

出典と根拠

ORDレコード: ord-8c091bc563e240e09933d3c61c1f3095
出典データセット: uspto-grants-1997_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05670527

反応ノート

読み込み中…