化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Acetate → 1,7-Diphenyl-4-heptanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acetate | HCID 8857 | — |
| 反応物 | 1.7-Diphenylheptan-4-one | HCID 15352829 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | 1,7-Diphenyl-4-heptanol | HCID 10539870 | 30% |
反応手順
Using the procedure of Example 42 with the resultant compound of Example 52 gave, after silica gel chromatography using 15% ethyl acetate in hexane, the desired compound (Rf 0.23, 30% ethyl acetate in hexane) as an oil. 1H NMR (CDCl3) δ 1.4-1.8 (m, 8H), 2.62 (br t, 4 H), 3.63 (m, 1H), 7.15-7.3 (m, 10H). Mass spectrum (M+NH4)+ =286.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05670675 |
| 出典データセット | uspto-grants-1997_09 |
| ORD ID | ord-8d4a03d515a04174a37ab7e235e217d4 |
| 出典メモ | uspto-grants-1997_09 |