化工社化工社 化学情報印刷レポート · 研究参考用
1-Isocyanato-4-methoxybenzene → Carbamic acid,(4-methoxyphenyl)-,1h-indol-7-yl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Isocyanato-4-methoxybenzene | HCID 79443 | — |
| 反応物 | 7-Hydroxyindole | HCID 2737651 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | Carbamic acid,(4-methoxyphenyl)-,1h-indol-7-yl ester | HCID 20242122 | — |
反応手順
To a solution of 7-hydroxyindole (0.7 g.) in ethyl ether (25 ml) and triethylamine (1 ml) is added 0.8 g. 4-methoxyphenyl isocyanate (Aldrich 23860-0). The reaction is stirred for 3 days at room temperature. The solvent is removed in vacuo and the remaining oil is purified by HPLC on silica gel.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04579865 |
| 出典データセット | uspto-grants-1986_04 |
| ORD ID | ord-0d3d79ab1fce4551a70c6636a84fdf01 |
| 出典メモ | uspto-grants-1986_04 |