HCID 23325188、化合物 → 4-Aminohex-5-ynoic acid hydrochloride

HRID 1380484ノート

反応式

HRID 1380484 の反応式
[ClH:1].[NH2:2][CH:3]([C:11]#[CH:12])[CH2:4][CH2:5][C:6]([O:8]CC)=[O:7]>Cl>[ClH:1].[NH2:2][CH:3]([C:11]#[CH:12])[CH2:4][CH2:5][C:6]([OH:8])=[O:7]

参加物

3

反応物 1

HCID 23325188HCID 23325188、化合物

生成物 1

HCID 867407234-Aminohex-5-ynoic acid hydrochloride

試薬・触媒・溶媒 1

HCID 313Hydrochloric Acid溶媒

実験手順

A solution of 0.4 g of 1 in 2 ml of concentrated hydrochloric acid was stirred at room temperature for one hour. The water was evaporated. Toluene was added to the residue and distilled to remove residual water by azeotropic distillation. The residue was dried under reduced pressure to give 2, as a hygroscopic solid.

後処理

  1. customThe water was evaporated
  2. additionToluene was added to the residue
  3. distillationdistilled
  4. customto remove residual water
  5. distillationby azeotropic distillation
  6. customThe residue was dried under reduced pressure
  7. customto give 2

出典と根拠

ORDレコード
ord-120eef4f41cc4363a087d5da0525a238
出典データセット
uspto-grants-1986_04
特許番号
US04582529

反応ノート

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