Dimethylthiocarbamoyl chloride → HCID 53894584、化合物

HRID 1380836ノート

反応式

HRID 1380836 の反応式
[Cl:1][CH2:2][C:3]1[CH:8]=[C:7]([OH:9])[N:6]=[C:5]([CH3:10])[N:4]=1.[CH3:11][N:12]([CH3:16])[C:13](Cl)=[S:14]>>[CH3:11][N:12]([CH3:16])[C:13](=[S:14])[O:9][C:7]1[N:6]=[C:5]([CH3:10])[N:4]=[C:3]([CH2:2][Cl:1])[CH:8]=1

参加物

3

反応物 2

HCID 27871Dimethylthiocarbamoyl chlorideHCID 178433451HCID 178433451、化合物

生成物 1

HCID 53894584HCID 53894584、化合物

実験手順

4-Chloromethyl-6-hydroxy-2-methyl-pyrimidine is reacted with N,N-dimethylthiocarbamoyl chloride analogously to the process described in Example 86 in order to produce 4-chloromethyl-2-methyl-6-pyrimidinyl N,N-dimethylthiocarbamate which is required as the starting material in Example 30. This product is obtained in the form of a yellow oil.

出典と根拠

ORDレコード
ord-4da97e024df44118840f5afe7034730c
出典データセット
uspto-grants-1986_04
特許番号
US04584295

反応ノート

読み込み中…