Triethylamine → HCID 23323498、化合物

HRID 1381132ノート

反応式

HRID 1381132 の反応式
[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][C:11]2[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=2[C:13]([NH2:15])=O)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].C(N(CC)CC)C>>[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][C:11]2[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=2[C:13]#[N:15])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]

参加物

3

反応物 2

HCID 8471TriethylamineHCID 54259173HCID 54259173、化合物

生成物 1

HCID 23323498HCID 23323498、化合物

実験手順

3,85 g (15 mMol) of 2-(3-Nitrophenylamino)benzoic acid amide in 30 ml (0,325 Mol) phosphorooxychloride were treated with 4,32 ml (31 mMol) triethylamine which is added dropwise, whereby the reaction mixture warms up. After thirty minutes the excess of phosphorooxychloride is distilled off, the residue is treated with water and the solid product is filtered off.

後処理

  1. additionis added dropwise
  2. distillationAfter thirty minutes the excess of phosphorooxychloride is distilled off
  3. additionthe residue is treated with water
  4. filtrationthe solid product is filtered off

出典と根拠

ORDレコード
ord-9169ece5721a40f1a816b90af66ae9d8
出典データセット
uspto-grants-1986_04
特許番号
US04585772

反応ノート

読み込み中…