Hydrochloric Acid → HCID 178479216、化合物

HRID 1381351ノート

反応式

HRID 1381351 の反応式
C([NH:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 178474793HCID 178474793、化合物

生成物 1

HCID 178479216HCID 178479216、化合物

実験手順

A mixture of 1-(3-acetamidopropyl)-1H-tetrazole-5-thiol (85 g) and 6N hydrochloric acid (1 l) was refluxed for 75 minutes under stirring. The reaction mixture was concentrated in vacuo and precipitates were collected by filtration and washed with hexane and diethyl ether to give 1-(3-aminopropyl)-1H-tetrazole-5-thiol hydrochloride (67.15 g).

後処理

  1. temperaturewas refluxed for 75 minutes
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customprecipitates
  4. filtrationwere collected by filtration
  5. washwashed with hexane and diethyl ether

出典と根拠

ORDレコード
ord-43af6b268b6746e5b06c6e3873fd9716
出典データセット
uspto-grants-1986_04
特許番号
US04585872

反応ノート

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