gamma-Cyclodextrine → Icosapent

HRID 1381482

反応式

HRID 1381482 の反応式
C(O)[C@H]1O[C@@H]2O[C@H]3[C@H](O)[C@@H](O)[C@@H](O[C@H]4[C@H](O)[C@@H](O)[C@@H](O[C@H]5[C@H](O)[C@@H](O)C(O[CH:36]6[C@H:41](O)[C@@H:40](O)[CH:39]([CH:44]7[C@H:49](O)[C@@H:48](O)[CH:47]([O:52][C@H]8[C@H](O)[C@@H](O)[C@@H](O[C@H]9[C@H](O)[C@@H](O)[C@@H](O[C@H]1[C@H](O)[C@H]2O)O[C@@H]9CO)O[C@@H]8CO)[O:46][C@@H]7CO)O[C@@H:37]6[CH2:77]O)O[C@@H]5CO)O[C@@H]4CO)O[C@@H]3CO>C(O)[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O>[CH3:77][CH2:37]/[CH:36]=[CH:41]\[CH2:40]/[CH:39]=[CH:44]\[CH2:49]/[CH:48]=[CH:47]\[CH2:77]/[CH:37]=[CH:36]\[CH2:41]/[CH:40]=[CH:39]\[CH2:44][CH2:49][CH2:48][C:47]([OH:46])=[O:52]

参加物

3

反応物 1

HCID 44431027gamma-Cyclodextrine

生成物 1

HCID 446284Icosapent

試薬・触媒・溶媒 1

HCID 6255beta-Maltose溶媒2 回

実験手順

Four parts of gamma-cyclodextrin powder was dissolved in 100 parts of an aqueous maltose solution, maltose content of 96.5%, d.s.b., moisture content of 18%, and the solution was mixed with 4 parts of eicosapentaenoic triglyceride and a beta-maltose hydrate seed. The mixture was crystallized, solidified, aged, pulverized and dehydrated by the method in Example 3.

後処理

  1. customThe mixture was crystallized

出典と根拠

ORDレコード
ord-abe61f4ee30246cfbfb6d138254b60ad
出典データセット
uspto-grants-1989_02
特許番号
US04803077

関連ノート

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