Sodium ethoxide → HCID 178489578、化合物
反応式
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10]1[CH2:14][CH2:13][N:12](S(C2C=CC(C)=CC=2)(=O)=O)[N:11]=1.[O-]CC.[Na+]>O>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10]1[CH:14]=[CH:13][NH:12][N:11]=1参加物
4
実験手順
The product of step (a) (7.5 g) was added to a solution of sodium ethoxide (60 ml, prepared from 0.6 g sodium), at a temperature of 60°. The mixture was refluxed for 10 minutes, cooled, added to water, extracted with ethyl acetate, dried and evaporated to give the sub-title compound as a purple oil, ms 189 (M+).
後処理
- temperatureThe mixture was refluxed for 10 minutes
- temperaturecooled
- extractionextracted with ethyl acetate
- customdried
- customevaporated
出典と根拠
- ORDレコード
- ord-52fba63b6f094fad8d0e0627c77951d2
- 出典データセット
- uspto-grants-1989_02
- 特許番号
- US04803216
反応ノート
読み込み中…