化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Carbonate → 9-(1,3-Di-n-octanoyloxy-2-propoxymethyl)guanine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 9-(1,3-di-n-octanoyloxy-2 propoxymethyl)guanine HCl | HCID 136332160 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 9-(1,3-Di-n-octanoyloxy-2-propoxymethyl)guanine | HCID 136332159 | — |
反応手順
1.0 g of 9-(1,3-di-n-octanoyloxy-2 propoxymethyl)guanine HCl suspended in 50 ml of ether is stirred with a twofold stoichiometric excess of dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 9-(1,3-di-n-octanoyloxy-2-propoxy methyl)guanine as the free base.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04803271 |
| 出典データセット | uspto-grants-1989_02 |
| ORD ID | ord-db6385784dc245b09772589e1cf94e65 |
| 出典メモ | uspto-grants-1989_02 |