Sulfuric Acid → Sulfuric acid--aniline (1/1)
反応式
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:8](=[O:12])(=[O:11])([OH:10])[OH:9]>>[S:8]([OH:12])([OH:11])(=[O:10])=[O:9].[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
3
実験手順
In the dry processes, aniline and sulfuric acid, in substantially equimolar amounts are charged to the reactor to form aniline hydrogen sulfate therein. When the charging is completed, the temperature within the surrounding furnace is raised to heat the reactor and its contents above the rearrangement temperature. The released water is vented and is externally condensed.
出典と根拠
- ORDレコード
- ord-f261cff6c3d14c709307165936918e9a
- 出典データセット
- uspto-grants-1989_02
- 特許番号
- US04808342
反応ノート
読み込み中…