Sulfuric Acid → Sulfuric acid--aniline (1/1)

HRID 1382669ノート

反応式

HRID 1382669 の反応式
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:8](=[O:12])(=[O:11])([OH:10])[OH:9]>>[S:8]([OH:12])([OH:11])(=[O:10])=[O:9].[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

3

実験手順

In the dry processes, aniline and sulfuric acid, in substantially equimolar amounts are charged to the reactor to form aniline hydrogen sulfate therein. When the charging is completed, the temperature within the surrounding furnace is raised to heat the reactor and its contents above the rearrangement temperature. The released water is vented and is externally condensed.

出典と根拠

ORDレコード
ord-f261cff6c3d14c709307165936918e9a
出典データセット
uspto-grants-1989_02
特許番号
US04808342

反応ノート

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