HCID 21273330、化合物 → HCID 14372147、化合物
反応式
S([C:5]1[O:13][C:12]2[CH:11]=[C:10](C)[NH:9][C:8](=[O:15])[C:7]=2[CH:6]=1)(=O)(=O)N.O1C=CC=[C:17]1C(C)=CC(O)=O.O1C=CC=C1C=C(C)C(O)=O>>[CH3:17][C:11]1[C:12]2[O:13][CH:5]=[CH:6][C:7]=2[C:8](=[O:15])[NH:9][CH:10]=1参加物
4
実験手順
The title compound was prepared according to the procedure described for 2-sulfamoyl-6-methylfuro[3.2-c]pyridin-4-(5H)-one (Example 12 Step A) except 3-(2-furanyl)-3-methylacrylic acid was substituted for 3-(2-furanyl)methacrylic acid. Title compound was obtained in 41% yield, m.p. 239°-241° C., after crystallization from methanol.
後処理
- customThe title compound was prepared
出典と根拠
- ORDレコード
- ord-883d592244404fceadbf46d0f3f1ab4a
- 出典データセット
- uspto-grants-1989_02
- 特許番号
- US04808595
反応ノート
読み込み中…